四川矿区典型煤层地应力场瓦斯渗透性规律实验研究

在深部开采或复杂地质条件下,地应力对煤岩渗透率的影响明显,进而影响煤矿瓦斯抽采的效果。对四川矿区不同典型煤层条件下的原煤进行了实验研究,分析矿区典型地应力特征条件下煤岩渗透率的变化规律,拟合了煤岩渗透率与有效应力的函数关系模型。研究发现:煤岩的渗透率与有效应力呈规律性的反比例关系,并存在拐点。这一发现为该矿区根据地应力条件进行煤层强化增透措施选取提供了依据,该研究成果在四川矿区白皎煤矿的保护层开采应用中取得了较好的效果,瓦斯抽采效果良好。     

Differences between internal and external hydrogen effects on slow strain rate tensile test of iron-based superalloy A286

To investigate the evaluation method of hydrogen compatibility of A286 superalloy in high pressure hydrogen gas, SSRT tests of hydrogen-charged specimens were conducted at ambient temperature at various strain rates. The relative reduction in area (RRA), one of the ductility parameters, was determined. The hydrogen content in the hydrogen-charged specimen was the same as the equilibrium hydrogen content on the specimen surface at 150 °C in 70 MPa hydrogen gas. The strain rate dependence of RRA was smaller than that of RRA obtained in 70 MPa hydrogen gas at 150 °C. All the hydrogen-charged specimens showed slip-plane fractures in the grains in their cores. However, the specimens in 70 MPa hydrogen gas at 150 °C showed fracture surfaces morphology ranging from dimples to quasi-cleavages and intergranular fractures with decreasing strain rate. These dissimilarities are expected to arise from differences in the hydrogen concentration behaviors of the specimens during the deformation process.     

A graphical method of presenting property rights,building types,and residential behaviors: A case study of Xiaoxihu historic area,Nanjing

One of the main reasons for the decline of urban historic areas in China is the co-existence of multiple property rights. It also deeply affects conservation and regeneration practice. This paper aims to propose a graphical method that illustrates the association between property rights, space, and resident behavior. Based on typological maps and justified graphs, a three-step method was proposed to visualize the relationships between these three elements. The final graph and quantitative data were used to observe the evolution of the courtyard building from a diachronic perspective, as well as to compare the residential behavior in different types from a synchronic perspective. The results show that following the subdivision of property rights, the building layout become more diverse due to various illegal additions, while the residential behavior within different building types tends to be consistent. Moreover, the study observed the traditional Chinese courtyard buildings’ adaptability. The findings contribute to understand the evolution of Chinese urban historic areas and internal motivation, and provide guidance for the conservation and regeneration practice.     

Oxygen vacancies as a link between the grain growth and grain boundary conductivity anomalies in titanium-rich strontium titanate

Titanium-rich (Sr/Ti?=?0.995) strontium titanate (ST) ceramics, air-sintered in a temperature range of 1400–1625?°C, were reported to possess anomalies in the grain growth and analogous anomalies in the grain boundary (GB) conductivity activation energy. However, these two interface-related phenomena, occurring at GBs, could not be associated with each other using a simple “brick-layer” model. In this work we revise the topic and advocate that the deviation from the model comes from the oxygen vacancies localized at GBs of the rapidly-cooled ST ceramics. To verify this, we annealed the ceramics in oxygen and performed their systematic and comparative analysis using impedance spectroscopy. A levelling-off in the GB conductivity activation energy, which increases for ≤1.24?eV, and a four-fold decrease in the GB permittivity are observed after annealing. Thus, we confirm a key role of oxygen vacancies in relation between the grain growth and GB conductivity anomalies of as-sintered Ti-rich ST ceramics.     

Mullite-bonded SiC-whisker-reinforced SiC matrix composites: Preparation,characterization, and toughening mechanisms

A novel mullite-bonded SiC-whisker-reinforced SiC matrix composite (SiCw/SiC, SiC whisker-to-SiC powder mass ratio of 1:9) was designed and successfully prepared. Before preparing the composite, the inexpensive lab-made SiCw was first modified by an oxidation/leaching process and then coated with Al₂O₃. The kinetics results indicate that the oxidation process can be described by improved shrinking-cylinder models. The aspect ratio of SiCw improved after modification. Subsequently, raw materials with a SiC–SiO₂–Al₂O₃ triple-layered structure were obtained after the Al₂O₃-coating process and used as feedstocks during the subsequent hot-pressing sintering. Finally, the characterization of the composites indicates that the mullite-bonded sample performs better (relative density of 93.8?±?1.4%, flexural strength of 533.3?±?18.2?MPa, fracture toughness of 13.6?±?2.1?MPa?m^1/2, and Vickers hardness of 20.6?±?2.5?GPa) than the reference sample without the mullite interface. The improved toughness could essentially be attributed to the moderately strong interface bonding and effective load transfer effects of the mullite interface.     

四川盆地高石梯-磨溪地区下二叠统气源示踪

以天然气、烃源岩及储层沥青的地球化学特征为主要依据,通过天然气-天然气、储层沥青-烃源岩、天然气-烃源岩3个方面对比,深入探讨四川盆地高石梯-磨溪地区下二叠统天然气来源。研究表明,四川盆地高石梯-磨溪地区下二叠统天然气主要来源于筇竹寺组泥岩。其5项证据分别为:下二叠统天然气乙烷碳同位素小于-30.5‰,甲、乙烷碳同位素倒转是由高演化程度烃源岩所致;多数下二叠统天然气与龙王庙组天然气特征最为相似;GS18,NC1井下二叠统天然气特征与寒武系相似,说明上下层气源一致;高石梯-磨溪地区下二叠统储层沥青地球化学特征与筇竹寺组泥岩最为相似;筇竹寺组泥岩主要为下二叠统供气,这一认识符合干酪根油气生成理论和同位素分馏规律。     

矿井顶板水探测方法及富水区成因分析

某矿1303工作面为三采区首采工作面，顶板含水层主要为第四系含水层、K₁₀和K₈砂岩裂隙含水层。为了解顶板K₁₀和K₈砂岩裂隙含水层的富水性，在1303工作面运输巷布置了覆盖全工作面的10个钻场（46个顶板探放水钻孔）进行探测，结合地表钻孔的顶板覆岩规律以及抽水试验结果可知，K₁₀和K₈砂岩裂隙含水层属于弱富水含水层，在2号钻场和8号钻场周边局部存在局部富水区；局部富水区均与构造有关，2号钻场位于背斜翼部，8号钻场位于向斜轴部，而背斜翼部和向斜轴部易出现砂岩裂隙带，成为地下水的富集区。     

近地表采空区处理及残矿开采技术研究与应用

某铅锌矿采用分段空场嗣后法开采,由于充填系统建设滞后导致近地表开采区域遗留大面积采空区及矿柱。针对采空区及残矿赋存现状,运用中深孔顶板及矿柱联合崩落的方式,崩落近地表采空区顶板隔离层及矿柱。采空区顶板及矿柱崩落后利用井下现有出矿系统集中出矿,出矿结束后对采空区进行充填。该技术方案有效消除采空区垮塌的安全隐患同时回采矿柱残矿,为同类矿山采空区处理及残矿回采提供技术参考。     

青海省祁连煤田石炭纪控煤构造及找煤远景区分析

石炭纪是青海省第一个成煤时代，在祁连山、柴北缘、唐古拉山等赋煤带均有分布。其中，祁连山赋煤带的祁连煤田晚石炭世羊虎沟组含煤地层分布面积最为广泛，含煤性较好，是青海省无烟煤重要产地，代表性煤矿有宁缠、青羊沟、阿力克、五林沟等。受成煤期后印支—燕山—喜山新构造运动的改造，使祁连煤田现今构造极为复杂，原含煤盆地被切割破坏成若干断块，有些地段被推覆构造掩盖，破坏了煤系及煤层的完整连续性，制约了在该区找煤的突破。为解决这一问题，从梳理总结祁连煤田上石炭统羊虎沟组岩性组合特征入手，通过分析北祁连成煤期后构造改造对煤系、煤层的控制作用，分析了几个典型的控煤构造样式，对找煤标志进行了归纳总结，指出了羊虎沟组在潟湖沉积体系内泥炭沼泽沉积层段含煤性最好，提出峨堡、阿力克深部、野牛台、小八宝等找煤远景区。     

双磁极式磁粒研磨机理分析及试验研究

目的解决平面磁粒研磨中压力不均匀和需要反复调整研磨间隙的问题,设计双磁极式研磨方法。方法首先对双磁极式研磨方法机理进行分析,并对研磨区域单颗磨粒进行受力分析,寻找影响研磨压力的主要因素;其次利用Ansoft Maxwell软件对两种研磨方法进行磁场仿真,分析两种研磨方法的研磨区域磁场梯度变化,通过面积积分法对比磁感应强度的影响程度;最后设计试验装置,通过试验对理论分析及有限元分析的结果进行验证,对比研磨前后工件表面粗糙度及微观形貌变化。结果双磁极式研磨方法中磨粒的研磨压力完全由磁场力提供,与研磨区域磁感应强度成正比,研磨区域磁感应强度比"铣削式"研磨方法提高约34.56%。两种方法在相同试验条件下对SUS304不锈钢板研磨40 min,双磁极式研磨方法研磨后,工件表面原始纹理基本被去除,表面粗糙度值由原始的0.25μm下降至0.16μm,下降率为36%,比"铣削式"研磨方法提高约80%,粗糙度曲线波动平缓,波峰波谷高度差变化均匀且表面形貌光滑平整。结论双磁极式研磨方法研磨区域磁场梯度变化明显,利于磨粒流动更新,研磨压力相对稳定,表面粗糙度下降率高,研磨后工件表面形貌光整,与"铣削式"研磨方法相比具有较明显的优势。